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Dresden 2014 – wissenschaftliches Programm

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MM: Fachverband Metall- und Materialphysik

MM 27: Transport I - Materials/Methods

MM 27.2: Vortrag

Dienstag, 1. April 2014, 12:00–12:15, IFW B

Diffusion of Atoms and Vacancies in Thin Nano Crystalline Platinum Films — •Wolfgang Gruber1, Johanna Rahn1, Florian Strauss1, Lars Dörrer1, Erwin Hüger1, Michael Horisberger2, Thomas Geue2, Jochen Stahn2, Carsten Bähtz3, Wolfram Leitenberger4, and Harald Schmidt11TU Clausthal — 2Paul Scherrer Institut — 3Helmholtz-Zentrum Dresden-Rossendorf — 4Universität Potsdam

An important characteristic of thin metal films deposited on substrates is the presence of a high number of defects in the metal film which is correlated to residual stress and strain. During heat treatment strain in the metal films relaxes. The relative changes of the film thickness and the interplanar distance are correlated to the change of the defect concentration during relaxation. In-situ X-ray diffraction and X-ray reflectometry using synchrotron radiation revealed that strain relaxation is accompanied by an increase of the vacancy concentration at the surface of the film [1]. In this work we present experimental results supporting the stress relaxation model outlined in [1]. To clarify the rate determining process for strain relaxation, grain boundary and volume self-diffusion of platinum is investigated. Samples enriched in the stable isotope 194Pt as tracer source were prepared and used for analysis with secondary ion mass spectrometry and neutron reflectometry. [1] W. Gruber, S. Chakravarty, C. Baehtz, W. Leitenberger, M. Bruns, A. Kobler, C. Kübel, H. Schmidt, Phys. Rev. Lett. 117 (2011) 265501.

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