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O: Fachverband Oberflächenphysik

O 37: Poster 2D Materials Beyond Graphene: Growth, Structure and Substrate Interaction (joint session O/HL)

O 37.5: Poster

Tuesday, March 18, 2025, 13:30–15:30, P3

UHV-CVD on Ir(111) for the Growth of 2D Materials — •Niels Ganser1, Marko Kriegel1, Karim Omambac1, Marin Petrovic2, Christian Brand1, Steffen Franzka3, Birk Finke1, Tobias Hartl4, Thomas Michely4, Frank-Joachim Meyer zu Heringdorf1, and Michael Horn-von Hoegen11Universität Duisburg-Essen — 2Institute of Physics, Zagreb — 3ICAN, Duisburg — 4Universität zu Köln

Hexagonal boron nitride (hBN) can be grown by scalable chemical vapor deposition (CVD) from a borazine B3N3H6 precursor. Here we show that the hBN quality depends strongly on the growth temperature Tg and the dosing pressure p.

Combined SPA-LEED and LEEM measurements show a strong dependence of n on p. We find that the quality of the hBN layers that can be achieved by increasing Tg is limited by the process of disintegration of the borazine at Tg> 950 C resulting in growth of borophene (2D Boron) instead [1]. Thus, it is possible to selectively grow either hBN or borophene from the same precursor [2].

Corroborating SPA-LEED measurements reveal a negative thermal expansion coefficient of α = (−2.4 ± 1.2) × 10−6 K−1 for 2D hBN in the temperature regime between 700 and 1100 C. This finding can be explained by Lifshitz’ membrane effect [3].

[1] Lifshitz, I., Zh. Eksp. Teor. Fiz. 22, 475 (1952)

[2] Omambac, K. et al., ACS Nano 15, 7421 (2021)

[3] Omambac, K. et al., ACS Nano 17, 17946 (2023)

Keywords: hexagonal boron nitride; chemical vapor deposition; selective growth

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